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Radiation hardness testing allows you to test the effect of neutron
radiation on materials, components, instruments and biological specimens.
This procedure is also used to harden the components for use in
applications where they may be exposed to a neutron stream. These
applications include aerospace, telecommunications, electronics
and defense industries.
Neutron activation analysis, discovered in 1936, stands at the
forefront of techniques for the quantitative multi-element analysis
of major, minor, trace and rare elements. Advances in semiconductor
detector systems coupled with improvements in research reactors,
especially development of the reactor at the UCD MNRC, have done
much to aid the proliferation of the neutron activation analysis
technique. Today, instrumental neutron activation analysis is used
for diverse applications in studies requiring nondestructive analysis
of samples and/or low levels of sensitivity for the elements of
interest.
The principle involved in neutron activation analysis consists
of first irradiating a sample with neutrons in a nuclear reactor
to produce specific radionuclides. After the irradiation, the characteristic
gamma rays emitted by the decaying radionuclides are quantitatively
measured by gamma spectroscopy, where the gamma rays detected at
a particular energy are indicative of a specific radionuclide's
presence. Data reduction of gamma ray spectra then yields the concentrations
of various elements in the samples being studied. With instrumental
neutron activation analysis it is possible to measure quantitatively
about 60 activatable elements in small samples. The lower limit
of detection is on the order of parts per million to parts per billion
depending on the element analyzed and the activity of the bulk sample
matrix.
The following table gives a list of elements that may be quantitatively
analyzed using neutron activation analysis:
|
| Aluminum |
Antimony |
Arsenic |
Barium |
|
| Cadmium |
Cerium |
Cesium |
Chlorine |
|
| Chromium |
Cobalt |
Copper |
Dysprosium |
|
| Erbium |
Europium |
Gadolinium |
Gallium |
|
| Germanium |
Gold |
Hafnium |
Indium |
|
| Iodine |
Iridium |
Iron |
Lanthanum |
|
| Lutetium |
Magnesium |
Manganese |
Mercury |
|
| Molybdenum |
Neodymium |
Nickel |
Niobium |
|
| Osmium |
Palladium |
Platinum |
Potassium |
|
| Praseodymium |
Rhenium |
Rubidium |
Ruthenium |
|
| Samarium |
Scandium |
Selenium |
Silver |
|
| Sodium |
Strontium |
Tantalum |
Tellurium |
|
| Terbium |
Thorium |
Thulium |
Tin |
|
| Titanium |
Tungsten |
Uranium |
Vanadium |
|
| Ytterbium |
Zinc |
Zirconium |
|
|
Applications of NAA
MNRC's neutron activation analysis laboratory was designed to analyze
for the major, minor, and trace element content of samples covering
a wide spectrum of material types and involving many scientific
and technical fields. MNRC can provide neutron activation analysis
services for a wide range of customers. Included in this service
is: sample preparation, sequential irradiation and counting, data
reduction and analysis, and report preparation. This technique is
particularly useful for forensics in crime analysis, accident analysis,
and other uses. The following list includes some of the scientific,
engineering, and industrial disciplines that can benefit from the
use of neutron activation analysis at the MNRC and the types of
material analyzed:
|
| Agriculture |
beet pulp, lipids, hay, oil, fish |
|
| Anthropology |
obsidian, teeth, bones |
|
| Archeology |
pottery sherds, clay samples |
|
| Biology |
chemicals, sugar, enzymes, solutions, ants |
|
| Botany |
wheat spores |
|
| Chemistry |
oxides, salts, pure crystals, and metals
residue swabs |
|
| Corning Glass, Inc. |
raw materials for the production of optical
glass |
|
| Engineering & Industry |
pure metals, chemical compounds, oils, thin
film deposits, plastic films, alloys, rocks |
|
| Fisheries |
fish, shells |
|
| Forensics |
bullets, paint, glass, metals, gunshot residue
swabs |
|
| Forestry |
wood, phloem, tree needles, soil |
|
| Geology |
basaltic rocks, soil assays, meteorites,
gems, minerals |
|
| Materials Science & Engineering |
silicon based materials |
|
| Medicine |
water, skin, hair, nails |
|
| Nuclear Industry |
electronics packages for radiation sensing
devices |
|
| Oceanography |
fossils, sediments, basalts |
|
| Pharmacy |
chemicals |
|
| Textiles |
fabrics, other textiles |
|
Research Isotopes
A variety of research isotopes can be produced at MNRC upon demand
utilizing a neutron flux up to 4 x 1013 n/cm2·s,
including but not limited to:
|
|
|
| Argon-41 |
|
|
|
| Cadmium-109 |
|
|
|
| Calcium-41 |
|
|
|
| Holmium-166 |
|
|
|
| Iodine-125 |
|
|
|
| Iridium-192 |
|
|
|
| Iron-59 |
|
|
|
| Lutetium-177 |
|
|
|
| Samarium-153 |
|
|
|
| Selenium-75 |
|
|
|
| Xenon-127 |
|
|
|
| Yttrium-90 |
|
|
|
|
|
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Our unique reactor configuration facilitates flexible power irradiation
runs making MNRC the ideal research isotope production partner.
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